SnO2/CNT composites were prepared by microwave assisted wet impregnation at 60 °C. The process was optimized by varying the microwave power and reaction time. Raman analysis showed the typical features of the rutile phase of as-synthesized SnO2 nanoparticles on CNTs, which was consistent with the results from X-ray diffraction. Enhanced field emission performance was observed for SnO2/CNT composite prepared by a microwave method when compared to pure CNTs and SnO2/CNT prepared by conventional wet impregnation. The dependence of emission current density on the electric field followed a Fowler–Nordheim relationship.
Reference:
Kesavan Pillai, S., Motshekga, S.C., Ray, S.S. and Kennedy, J. 2012. Field emission characteristics of SnO2/CNT composite prepared by microwave assisted wet impregnation. Journal of Nanomaterials (2012), pp 1-8
Kesavan Pillai, S., Motshekga, S., Ray, S., & Kennedy, J. (2012). Field emission characteristics of SnO2/CNT composite prepared by microwave assisted wet impregnation. http://hdl.handle.net/10204/5498
Kesavan Pillai, Sreejarani, SC Motshekga, SS Ray, and J Kennedy "Field emission characteristics of SnO2/CNT composite prepared by microwave assisted wet impregnation." (2012) http://hdl.handle.net/10204/5498
Kesavan Pillai S, Motshekga S, Ray S, Kennedy J. Field emission characteristics of SnO2/CNT composite prepared by microwave assisted wet impregnation. 2012; http://hdl.handle.net/10204/5498.